{"product_id":"shigemi-nmr-tubes-solvent-matched","title":"Shigemi NMR tubes, 5 mm and 3 mm, solvent-matched","description":"\u003cdiv style=\"margin-bottom: 28px;\"\u003e\n\u003cdiv style=\"background: #002147; padding: 10px 20px; margin-bottom: 0;\"\u003e\u003ch3 style=\"margin: 0; font-family: 'Helvetica Neue', Helvetica, Arial, sans-serif; font-size: 0.70em; font-weight: 700; letter-spacing: 0.12em; text-transform: uppercase; color: #fff;\"\u003eWhat this tube is for\u003c\/h3\u003e\u003c\/div\u003e\n\u003cdiv style=\"padding: 16px 20px; border: 1px solid #e4e8f0; border-top: none; font-family: Georgia, 'Times New Roman', serif; font-size: 0.95em; line-height: 1.65; color: #333;\"\u003e\n\u003cp\u003eA Shigemi tube lets you record a good spectrum from much less sample than a normal tube needs. It is a set of two parts: an outer tube with a thick glass bottom, and a glass plunger that you lower onto the sample from above. Both pieces of glass are made to match the magnetic susceptibility of one solvent. To the magnet, the sample seems to continue above and below, so the field stays even and shimming works as with a full tube.\u003c\/p\u003e\n\u003cp\u003eThe result is that the whole sample sits in the detection region of the probe, at the highest concentration the sample allows. Typical uses: natural products, metabolites, proteins and peptides, and any compound that is expensive or available only in milligram amounts or less.\u003c\/p\u003e\n\u003c\/div\u003e\n\u003c\/div\u003e\u003cdiv style=\"margin-bottom: 28px;\"\u003e\n\u003cdiv style=\"background: #002147; padding: 10px 20px; margin-bottom: 0;\"\u003e\u003ch3 style=\"margin: 0; font-family: 'Helvetica Neue', Helvetica, Arial, sans-serif; font-size: 0.70em; font-weight: 700; letter-spacing: 0.12em; text-transform: uppercase; color: #fff;\"\u003eYour choices\u003c\/h3\u003e\u003c\/div\u003e\n\u003cdiv style=\"padding: 16px 20px; border: 1px solid #e4e8f0; border-top: none; font-family: Georgia, 'Times New Roman', serif; font-size: 0.95em; line-height: 1.65; color: #333;\"\u003e\n\u003cp\u003e\u003cstrong\u003eSize: 5 mm or 3 mm.\u003c\/strong\u003e Choose the size that your probe takes. The 5 mm tube fits any standard 5 mm probe and needs roughly half the liquid of a normal 5 mm tube. The 3 mm tube is for the smallest samples: its narrower bore needs even less liquid, but it needs a 3 mm probe, or a spinner that holds 3 mm tubes in a 5 mm probe. If you are not sure, choose 5 mm.\u003c\/p\u003e\n\u003cp\u003e\u003cstrong\u003eSpectrometer: Bruker or Varian (5 mm only).\u003c\/strong\u003e The 5 mm glass bottom is 8 mm long for Bruker probes and 15 mm for Varian probes. The receiver coil sits higher in a Varian probe than in a Bruker probe, so the Varian tube needs a longer glass bottom to lift the sample to the coil. Varian and Agilent NMR spectrometers take the Varian version. The 3 mm tube comes in one universal version with a 10 mm glass bottom, for Bruker and Varian probes alike, so there is nothing to choose.\u003c\/p\u003e\n\u003cp\u003e\u003cstrong\u003eChoose the right version: it protects your probe.\u003c\/strong\u003e A 5 mm Varian tube in a Bruker probe pushes its 15 mm glass bottom down into the coil region and can damage the probe. A 5 mm Bruker tube in a Varian probe does no harm, but the sample sits below the coil and the spectrum is poor. If you are not sure which probe you have, ask us before ordering.\u003c\/p\u003e\n\u003cp\u003e\u003cstrong\u003eSolvent.\u003c\/strong\u003e Choose the tube matched to the solvent you will use: D₂O, CDCl₃, DMSO-d₆, CD₃OD or acetone-d₆. The DMSO-d₆ tube also suits pyridine-d₅ and benzene-d₆, and the CD₃OD tube also suits acetonitrile-d₃, because their susceptibilities are close. A tube used with the wrong solvent gives distorted lineshapes.\u003c\/p\u003e\n\u003cp\u003e\u003cstrong\u003eThe most common choice is CMS-005B:\u003c\/strong\u003e the 5 mm CDCl₃ tube for Bruker instruments.\u003c\/p\u003e\n\u003c\/div\u003e\n\u003c\/div\u003e\u003cdiv style=\"margin-bottom: 28px;\"\u003e\n\u003cdiv style=\"background: #002147; padding: 10px 20px; margin-bottom: 0;\"\u003e\u003ch3 style=\"margin: 0; font-family: 'Helvetica Neue', Helvetica, Arial, sans-serif; font-size: 0.70em; font-weight: 700; letter-spacing: 0.12em; text-transform: uppercase; color: #fff;\"\u003eTechnical specifications\u003c\/h3\u003e\u003c\/div\u003e\n\u003ctable style=\"width: 100%; table-layout: auto; border-collapse: collapse; font-size: 0.95em; border: 1px solid #e4e8f0; border-top: none; font-family: 'Helvetica Neue', Helvetica, Arial, sans-serif;\"\u003e\n\u003cthead\u003e\u003ctr\u003e\n\u003cth style=\"padding: 9px 8px; text-align: left; font-weight: 600; color: #002147; background: #f7f8fb; border-bottom: 1px solid #e4e8f0;\"\u003eItem no.\u003c\/th\u003e\n\u003cth style=\"padding: 9px 8px; text-align: left; font-weight: 600; color: #002147; background: #f7f8fb; border-bottom: 1px solid #e4e8f0;\"\u003eMatched to\u003c\/th\u003e\n\u003cth style=\"padding: 9px 8px; text-align: left; font-weight: 600; color: #002147; background: #f7f8fb; border-bottom: 1px solid #e4e8f0;\"\u003eVersion\u003c\/th\u003e\n\u003c\/tr\u003e\u003c\/thead\u003e\n\u003ctbody\u003e\n\u003ctr style=\"background: #eef5fb;\"\u003e\n\u003ctd style=\"padding: 9px 8px; border-bottom: 1px solid #e4e8f0; color: #002147; font-weight: 600;\"\u003e\u003cspan style=\"white-space: nowrap;\"\u003eCMS-005B\u003c\/span\u003e\u003c\/td\u003e\n\u003ctd style=\"padding: 9px 8px; border-bottom: 1px solid #e4e8f0; color: #333;\"\u003eCDCl₃\u003c\/td\u003e\n\u003ctd style=\"padding: 9px 8px; border-bottom: 1px solid #e4e8f0; color: #333;\"\u003e5 mm, Bruker, bottom 8 mm\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd style=\"padding: 9px 8px; border-bottom: 1px solid #e4e8f0; color: #002147; font-weight: 600;\"\u003e\u003cspan style=\"white-space: nowrap;\"\u003eDMS-005B\u003c\/span\u003e\u003c\/td\u003e\n\u003ctd style=\"padding: 9px 8px; border-bottom: 1px solid #e4e8f0; color: #333;\"\u003eDMSO-d₆ (also pyridine-d₅, C₆D₆)\u003c\/td\u003e\n\u003ctd style=\"padding: 9px 8px; border-bottom: 1px solid #e4e8f0; color: #333;\"\u003e5 mm, Bruker, bottom 8 mm\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd style=\"padding: 9px 8px; border-bottom: 1px solid #e4e8f0; color: #002147; font-weight: 600;\"\u003e\u003cspan style=\"white-space: nowrap;\"\u003eBMS-005B\u003c\/span\u003e\u003c\/td\u003e\n\u003ctd style=\"padding: 9px 8px; border-bottom: 1px solid #e4e8f0; color: #333;\"\u003eD₂O\u003c\/td\u003e\n\u003ctd style=\"padding: 9px 8px; border-bottom: 1px solid #e4e8f0; color: #333;\"\u003e5 mm, Bruker, bottom 8 mm\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd style=\"padding: 9px 8px; border-bottom: 1px solid #e4e8f0; color: #002147; font-weight: 600;\"\u003e\u003cspan style=\"white-space: nowrap;\"\u003eMMS-005B\u003c\/span\u003e\u003c\/td\u003e\n\u003ctd style=\"padding: 9px 8px; border-bottom: 1px solid #e4e8f0; color: #333;\"\u003eCD₃OD (also acetonitrile-d₃)\u003c\/td\u003e\n\u003ctd style=\"padding: 9px 8px; border-bottom: 1px solid #e4e8f0; color: #333;\"\u003e5 mm, Bruker, bottom 8 mm\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd style=\"padding: 9px 8px; border-bottom: 1px solid #e4e8f0; color: #002147; font-weight: 600;\"\u003e\u003cspan style=\"white-space: nowrap;\"\u003eAMS-005B\u003c\/span\u003e\u003c\/td\u003e\n\u003ctd style=\"padding: 9px 8px; border-bottom: 1px solid #e4e8f0; color: #333;\"\u003eAcetone-d₆\u003c\/td\u003e\n\u003ctd style=\"padding: 9px 8px; border-bottom: 1px solid #e4e8f0; color: #333;\"\u003e5 mm, Bruker, bottom 8 mm\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd style=\"padding: 9px 8px; border-bottom: 1px solid #e4e8f0; color: #002147; font-weight: 600;\"\u003e\u003cspan style=\"white-space: nowrap;\"\u003eCMS-005V\u003c\/span\u003e\u003c\/td\u003e\n\u003ctd style=\"padding: 9px 8px; border-bottom: 1px solid #e4e8f0; color: #333;\"\u003eCDCl₃\u003c\/td\u003e\n\u003ctd style=\"padding: 9px 8px; border-bottom: 1px solid #e4e8f0; color: #333;\"\u003e5 mm, Varian, bottom 15 mm\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd style=\"padding: 9px 8px; border-bottom: 1px solid #e4e8f0; color: #002147; font-weight: 600;\"\u003e\u003cspan style=\"white-space: nowrap;\"\u003eDMS-005V\u003c\/span\u003e\u003c\/td\u003e\n\u003ctd style=\"padding: 9px 8px; border-bottom: 1px solid #e4e8f0; color: #333;\"\u003eDMSO-d₆ (also pyridine-d₅, C₆D₆)\u003c\/td\u003e\n\u003ctd style=\"padding: 9px 8px; border-bottom: 1px solid #e4e8f0; color: #333;\"\u003e5 mm, Varian, bottom 15 mm\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd style=\"padding: 9px 8px; border-bottom: 1px solid #e4e8f0; color: #002147; font-weight: 600;\"\u003e\u003cspan style=\"white-space: nowrap;\"\u003eBMS-005V\u003c\/span\u003e\u003c\/td\u003e\n\u003ctd style=\"padding: 9px 8px; border-bottom: 1px solid #e4e8f0; color: #333;\"\u003eD₂O\u003c\/td\u003e\n\u003ctd style=\"padding: 9px 8px; border-bottom: 1px solid #e4e8f0; color: #333;\"\u003e5 mm, Varian, bottom 15 mm\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd style=\"padding: 9px 8px; border-bottom: 1px solid #e4e8f0; color: #002147; font-weight: 600;\"\u003e\u003cspan style=\"white-space: nowrap;\"\u003eMMS-005V\u003c\/span\u003e\u003c\/td\u003e\n\u003ctd style=\"padding: 9px 8px; border-bottom: 1px solid #e4e8f0; color: #333;\"\u003eCD₃OD (also acetonitrile-d₃)\u003c\/td\u003e\n\u003ctd style=\"padding: 9px 8px; border-bottom: 1px solid #e4e8f0; color: #333;\"\u003e5 mm, Varian, bottom 15 mm\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd style=\"padding: 9px 8px; border-bottom: 1px solid #e4e8f0; color: #002147; font-weight: 600;\"\u003e\u003cspan style=\"white-space: nowrap;\"\u003eAMS-005V\u003c\/span\u003e\u003c\/td\u003e\n\u003ctd style=\"padding: 9px 8px; border-bottom: 1px solid #e4e8f0; color: #333;\"\u003eAcetone-d₆\u003c\/td\u003e\n\u003ctd style=\"padding: 9px 8px; border-bottom: 1px solid #e4e8f0; color: #333;\"\u003e5 mm, Varian, bottom 15 mm\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd style=\"padding: 9px 8px; border-bottom: 1px solid #e4e8f0; color: #002147; font-weight: 600;\"\u003e\u003cspan style=\"white-space: nowrap;\"\u003eCMS-003\u003c\/span\u003e\u003c\/td\u003e\n\u003ctd style=\"padding: 9px 8px; border-bottom: 1px solid #e4e8f0; color: #333;\"\u003eCDCl₃\u003c\/td\u003e\n\u003ctd style=\"padding: 9px 8px; border-bottom: 1px solid #e4e8f0; color: #333;\"\u003e3 mm, Bruker and Varian, bottom 10 mm\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd style=\"padding: 9px 8px; border-bottom: 1px solid #e4e8f0; color: #002147; font-weight: 600;\"\u003e\u003cspan style=\"white-space: nowrap;\"\u003eDMS-003\u003c\/span\u003e\u003c\/td\u003e\n\u003ctd style=\"padding: 9px 8px; border-bottom: 1px solid #e4e8f0; color: #333;\"\u003eDMSO-d₆ (also pyridine-d₅, C₆D₆)\u003c\/td\u003e\n\u003ctd style=\"padding: 9px 8px; border-bottom: 1px solid #e4e8f0; color: #333;\"\u003e3 mm, Bruker and Varian, bottom 10 mm\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd style=\"padding: 9px 8px; border-bottom: 1px solid #e4e8f0; color: #002147; font-weight: 600;\"\u003e\u003cspan style=\"white-space: nowrap;\"\u003eBMS-003\u003c\/span\u003e\u003c\/td\u003e\n\u003ctd style=\"padding: 9px 8px; border-bottom: 1px solid #e4e8f0; color: #333;\"\u003eD₂O\u003c\/td\u003e\n\u003ctd style=\"padding: 9px 8px; border-bottom: 1px solid #e4e8f0; color: #333;\"\u003e3 mm, Bruker and Varian, bottom 10 mm\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd style=\"padding: 9px 8px; border-bottom: 1px solid #e4e8f0; color: #002147; font-weight: 600;\"\u003e\u003cspan style=\"white-space: nowrap;\"\u003eMMS-003\u003c\/span\u003e\u003c\/td\u003e\n\u003ctd style=\"padding: 9px 8px; border-bottom: 1px solid #e4e8f0; color: #333;\"\u003eCD₃OD (also acetonitrile-d₃)\u003c\/td\u003e\n\u003ctd style=\"padding: 9px 8px; border-bottom: 1px solid #e4e8f0; color: #333;\"\u003e3 mm, Bruker and Varian, bottom 10 mm\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd style=\"padding: 9px 8px; border-bottom: 1px solid #e4e8f0; color: #002147; font-weight: 600;\"\u003e\u003cspan style=\"white-space: nowrap;\"\u003eAMS-003\u003c\/span\u003e\u003c\/td\u003e\n\u003ctd style=\"padding: 9px 8px; border-bottom: 1px solid #e4e8f0; color: #333;\"\u003eAcetone-d₆\u003c\/td\u003e\n\u003ctd style=\"padding: 9px 8px; border-bottom: 1px solid #e4e8f0; color: #333;\"\u003e3 mm, Bruker and Varian, bottom 10 mm\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003c\/tbody\u003e\n\u003c\/table\u003e\n\u003cdiv style=\"padding: 12px 20px; border: 1px solid #e4e8f0; border-top: none; font-family: 'Helvetica Neue', Helvetica, Arial, sans-serif; font-size: 0.9em; color: #333;\"\u003e5 mm tubes: outer diameter 4.965 ± 0.010 mm. 3 mm tubes: outer diameter 3.00 ± 0.020 mm. Both sizes: outer tube 180 mm long, plunger 190 mm long. Each item is a pack of 5 sets, as Deutero supplies them; each set is one outer tube and one plunger. Deutero can supply other tubes from the Shigemi range on request. Spare cap CS-005 fits all 5 mm Shigemi tubes.\u003c\/div\u003e\n\u003c\/div\u003e\u003cdiv style=\"margin-bottom: 28px;\"\u003e\n\u003cdiv style=\"background: #002147; padding: 10px 20px; margin-bottom: 0;\"\u003e\u003ch3 style=\"margin: 0; font-family: 'Helvetica Neue', Helvetica, Arial, sans-serif; font-size: 0.70em; font-weight: 700; letter-spacing: 0.12em; text-transform: uppercase; color: #fff;\"\u003eManufacturer\u003c\/h3\u003e\u003c\/div\u003e\n\u003cdiv style=\"padding: 14px 20px; border: 1px solid #e4e8f0; border-top: none; font-family: 'Helvetica Neue', Helvetica, Arial, sans-serif; font-size: 0.95em; color: #333; display: flex; align-items: center; gap: 18px;\"\u003e\n\u003cimg src=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0954\/6357\/1793\/files\/deutero-logo.png?v=1793286803\" alt=\"Deutero GmbH, NMR Spectroscopy\" width=\"120\" height=\"49\" style=\"width: 120px; height: auto; flex: 0 0 auto;\"\u003e\u003cdiv\u003eShigemi tubes, supplied by Deutero GmbH, Kastellaun, Germany. NorrChemica is an authorised distributor of Deutero GmbH.\u003c\/div\u003e\n\u003c\/div\u003e\n\u003c\/div\u003e\u003cdiv style=\"margin-bottom: 28px; background: #eef5fb; border-left: 4px solid #2392c4; padding: 16px 20px; font-family: 'Helvetica Neue', Helvetica, Arial, sans-serif;\"\u003e\n\u003cdiv style=\"font-size: 0.70em; font-weight: 700; letter-spacing: 0.12em; text-transform: uppercase; color: #002147; margin-bottom: 6px;\"\u003eNo spectrometer?\u003c\/div\u003e\n\u003cdiv style=\"font-size: 0.95em; color: #333; line-height: 1.5;\"\u003eSend us the sample and we run the NMR: ¹H, ¹³C, ¹⁹F, ³¹P and ¹¹B.\u003c\/div\u003e\n\u003ca href=\"\/pages\/nmr-service\" style=\"display: inline-block; margin-top: 10px; background: #002147; color: #fff; text-decoration: none; font-weight: 700; font-size: 0.9em; padding: 8px 16px; border-radius: 4px;\"\u003eSee the NMR analysis service →\u003c\/a\u003e\n\u003c\/div\u003e","brand":"Deutero","offers":[{"title":"CMS-005B · 5 mm · CDCl₃ · Bruker · 5 sets · most common","offer_id":55538890637649,"sku":"CMS-005B","price":1590.34,"currency_code":"EUR","in_stock":true},{"title":"DMS-005B · 5 mm · DMSO-d₆ · Bruker · 5 sets","offer_id":55538890670417,"sku":"DMS-005B","price":1759.01,"currency_code":"EUR","in_stock":true},{"title":"BMS-005B · 5 mm · D₂O · Bruker · 5 sets","offer_id":55538890703185,"sku":"BMS-005B","price":1590.34,"currency_code":"EUR","in_stock":true},{"title":"MMS-005B · 5 mm · CD₃OD · Bruker · 5 sets","offer_id":55538890735953,"sku":"MMS-005B","price":1759.01,"currency_code":"EUR","in_stock":true},{"title":"AMS-005B · 5 mm · Acetone-d₆ · Bruker · 5 sets","offer_id":55538890768721,"sku":"AMS-005B","price":2289.12,"currency_code":"EUR","in_stock":true},{"title":"CMS-005V · 5 mm · CDCl₃ · Varian · 5 sets","offer_id":55538890801489,"sku":"CMS-005V","price":1590.34,"currency_code":"EUR","in_stock":true},{"title":"DMS-005V · 5 mm · DMSO-d₆ · Varian · 5 sets","offer_id":55538890834257,"sku":"DMS-005V","price":1759.01,"currency_code":"EUR","in_stock":true},{"title":"BMS-005V · 5 mm · D₂O · Varian · 5 sets","offer_id":55538890867025,"sku":"BMS-005V","price":1590.34,"currency_code":"EUR","in_stock":true},{"title":"MMS-005V · 5 mm · CD₃OD · Varian · 5 sets","offer_id":55538890899793,"sku":"MMS-005V","price":1759.01,"currency_code":"EUR","in_stock":true},{"title":"AMS-005V · 5 mm · Acetone-d₆ · Varian · 5 sets","offer_id":55538890932561,"sku":"AMS-005V","price":2289.12,"currency_code":"EUR","in_stock":true},{"title":"CMS-003 · 3 mm · CDCl₃ · Bruker and Varian · 5 sets","offer_id":55541528920401,"sku":"CMS-003","price":2048.16,"currency_code":"EUR","in_stock":true},{"title":"DMS-003 · 3 mm · DMSO-d₆ · Bruker and Varian · 5 sets","offer_id":55541528953169,"sku":"DMS-003","price":2048.16,"currency_code":"EUR","in_stock":true},{"title":"BMS-003 · 3 mm · D₂O · Bruker and Varian · 5 sets","offer_id":55541528985937,"sku":"BMS-003","price":2289.12,"currency_code":"EUR","in_stock":true},{"title":"MMS-003 · 3 mm · CD₃OD · Bruker and Varian · 5 sets","offer_id":55541529018705,"sku":"MMS-003","price":2048.16,"currency_code":"EUR","in_stock":true},{"title":"AMS-003 · 3 mm · Acetone-d₆ · Bruker and Varian · 5 sets","offer_id":55541529051473,"sku":"AMS-003","price":2289.12,"currency_code":"EUR","in_stock":true},{"title":"CS-005 · spare cap for 5 mm Shigemi tubes","offer_id":55538890965329,"sku":"CS-005","price":33.49,"currency_code":"EUR","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0954\/6357\/1793\/files\/shigemi-5mm-nmr-tube.png?v=1793283749","url":"https:\/\/www.norrchemica.com\/products\/shigemi-nmr-tubes-solvent-matched","provider":"NorrChemica","version":"1.0","type":"link"}