Deutero
5 mm precision NMR tubes, Boro 3.3 glass, 200–600 MHz
5 mm precision NMR tubes, Boro 3.3 glass, 200–600 MHz
Pack sizes & prices
| Pack size | Excl. VAT | Add to cart |
|---|---|---|
| d500-5-7 · 500 MHz · 7 in · pack of 5 · most common | €81,00€101,66 incl. VAT | |
| d200-5-7 · 200 MHz · 7 in · box of 100 | €579,60€727,40 incl. VAT | |
| d200-5-8 · 200 MHz · 8 in · box of 100 | €655,20€822,28 incl. VAT | |
| d200-5-9 · 200 MHz · 9 in · box of 100 | €831,60€1.043,66 incl. VAT | |
| d300-5-7 · 300 MHz · 7 in · pack of 5 | €45,36€56,93 incl. VAT | |
| d300-5-8 · 300 MHz · 8 in · pack of 5 | €49,14€61,67 incl. VAT | |
| d300-5-9 · 300 MHz · 9 in · pack of 5 | €59,22€74,32 incl. VAT | |
| d400-5-7 · 400 MHz · 7 in · pack of 5 | €65,52€82,23 incl. VAT | |
| d400-5-8 · 400 MHz · 8 in · pack of 5 | €70,56€88,55 incl. VAT | |
| d400-5-9 · 400 MHz · 9 in · pack of 5 | €80,64€101,20 incl. VAT | |
| d500-5-8 · 500 MHz · 8 in · pack of 5 | €86,94€109,11 incl. VAT | |
| d500-5-9 · 500 MHz · 9 in · pack of 5 | €100,80€126,50 incl. VAT | |
| d600-5-7 · 600 MHz · 7 in · pack of 5 | €144,90€181,85 incl. VAT | |
| d600-5-8 · 600 MHz · 8 in · pack of 5 | €161,28€202,41 incl. VAT | |
| d600-5-9 · 600 MHz · 9 in · pack of 5 | €182,70€229,29 incl. VAT |
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What this tube is for
5 mm NMR tubes made to a spectrometer grade, from 200 to 600 MHz, in Boro 3.3 borosilicate glass (ASTM type 1 class A) with a thin 0.38 mm wall. The 5 mm is the outer diameter of the tube (4.95 mm), the size that most NMR probes take. The length is given separately: 7 inches is 178 mm, 8 inches 203 mm, 9 inches 229 mm. Deutero describes them as robust and made for precise measurements in routine and high-field work. They come in three lengths: 7, 8 and 9 inches.
Class A glass. Boro 3.3 glass expands less with heat than the Boro 5.1 glass of the standard tubes: the names give the expansion, 3.3 against 5.1 millionths per kelvin.
For 800 MHz, see the precision tubes in Boro 5.1 glass. For routine spectra, the cheaper economy tubes are enough.
Your choices
Grade: 200, 300, 400, 500 or 600 MHz. The grade tells you how straight and round the tube is. Concentricity tells how even the wall is all round; camber tells how straight the tube is. Both get smaller as the grade goes up, from 25 and 25 µm at 200 MHz to 5 and 7 µm at 600 MHz. Choose the grade of your spectrometer, or a higher one. A higher grade spins more evenly and gives sharper lines; a lower grade on a high-field instrument can broaden them.
Length: 7, 8 or 9 inches. This is the length of the glass tube. 7 inches (178 mm) is the standard NMR tube length and fits most spectrometers and sample changers; if you are not sure, choose 7 inches. Choose 8 inches (203 mm) or 9 inches (229 mm) only if your spectrometer or sample changer uses them. Deutero makes other lengths on request; ask us if you need one.
Pack. The 200 MHz tubes come in boxes of 100; the 300 to 600 MHz tubes in packs of 5. Each tube comes with its cap; Deutero can supply the caps in a colour of your choice on request.
The most common choice is d500-5-7: the 500 MHz grade in the 7-inch length.
Technical specifications
| Item no. | Grade | OD (mm) | Concentricity / camber (µm) | Pack |
|---|---|---|---|---|
|
d200-5-7 d200-5-8 d200-5-9 |
200 MHz | 4.950 ± 0.030 | 25 / 25 | box of 100 |
|
d300-5-7 d300-5-8 d300-5-9 |
300 MHz | 4.950 ± 0.020 | 7 / 25 | pack of 5 |
|
d400-5-7 d400-5-8 d400-5-9 |
400 MHz | 4.950 ± 0.015 | 7 / 13 | pack of 5 |
|
d500-5-7 d500-5-8 d500-5-9 |
500 MHz | 4.950 ± 0.015 | 5 / 13 | pack of 5 |
|
d600-5-7 d600-5-8 d600-5-9 |
600 MHz | 4.950 ± 0.010 | 5 / 7 | pack of 5 |
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Further reading
Reading NMR spectra — a five-part series
Written by the chemists who interpret the spectra.
- Part 1 — Reading ¹H and ¹³C NMR
- Part 2 — Reading ¹⁹F, ³¹P and ¹¹B NMR
- Part 3 — Reading 2D NMR: COSY, HSQC and HMBC
- Part 4 — Quantitative NMR: how a purity figure is made
- Part 5 — ¹⁵N NMR: which nitrogen is alkylated, protonated or coordinated?
More in Analysis Notes.